BioXAS Spectroscopy

BioXAS - Side

 🟡 Closed for Mono Upgrade

BioXAS-Side is adequate for high concentration and ambient temperature samples. Please contact the beamline scientists for more information.

BioXAS-side beamline has a 5 mrad separation from the central line. The Side beamline is similar to the Main beamline and differs in some of the optical components as outlined below.

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Performance Figures

Source

22-poles (11-periods), 2.1 Tesla, Flat-top Wiggler


Energy Range

5-32 keV

Resolution (dE/E)

1 x 10^-4

Spot Size

3 mm x 0.5 mm (v x h ) @ 12 keV

Flux

1x10^11 @ 12k eV

Sample Environment

Cryostat

LN2 or LHe temperatures: 5x1 mm, 7x3 mm, 15x5mm

Sample Wheel

for samples, 5x 1mm, 7x3 mm.

Optics

M1 Mirror

water cooled, Toroidal 1 m Si, Rh coated, sagittal radius 33mm

Monochromator

LN2 cooled Si(220), phi= 0 or 90 deg, non-fixed exit.

M2 Mirror

Flat bent, vertically focusing 1.1 m Rh-coated

DBHR

for energies below 10keV; a double bounce harmonic rejection mirror ( C-Coated Si)

Instrumentation

Detectors

Ionization Chambers, PIPS, Canberra 32-element HPGe Solid Sate

Cryostat

Oxford Cryostat (10K or 80 K)

Other

Shutter and beam attenuation filter; Soller slits, fluorescence filters.

Reference wheel

automatic reference wheel

Data Acquisition

GUI based Data Acquisition Manager Software (AcquaMan) and Python Based

Automation Package (cls_bxs_control)

Automatic scan queuing available for multiple samples and/or multiple spots on the same sample

Athena, Larch and Viper for data analysis

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Typical achievable flux

The plot of energy vs flux shows the typical flux achievable in the whole operational energy range (5-32 keV) for the Side beamline. Note: the flux drops noticeably at the edges of the range, but it's still usable for samples with relatively high concentrations of the elements of interest.

Reference Foils

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Reference foil spectra captured on bioXAS-Side in transmission mode. The resolution is comparable to those reported in the literature for typical Spectroscopy Beamlines.